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LC-MS and LC-MS/MS analysis LC-MS and LC-MS/MS analysis was performed using an Agilent 6546 liquid chromatography/ quadrupole time-of-flight (LC/Q-TOF) mass spectrometer with an Agilent Jet Stream electrospray ionization (ESI) source coupled to an Agilent 1290 Infinity II ultra-high performance liquid chromatography (UHPLC) system
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